Chapter 6 HPLC
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ID： |
D3204F5E1AD940A6B111B099B2FAC937 |
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文件大小(MB)： |
0.33 |
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页数： |
82 |
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文件格式： |
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日期： |
2002-6-11 |
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购买： |
文本摘录（文本识别可能有误，但文件阅览显示及打印正常，pdf文件可进行文字搜索定位）：
Transmittal No. 96-E1 (9/96),Form FDA 2905a (6/92) 600–1,Pesticide Analytical Manual Vol. I SECTION 600,Table of Contents,page date,601: General Information,601 A: Principles 601-1 1/94,601 B: Modes of Operation 601-2 1/94,Liquid-Solid Chromatography 601-2 1/94,Liquid-Liquid Chromatography 601-3 1/94,Bonded Phase Chromatography 601-3 1/94,Ion Exchange Chromatography 601-4 1/94,Size Exclusion Chromatography 601-4 1/94,601 C: Instrumentation and Apparatus 601-5 1/94,Basic Components 601-5 1/94,601 D: Solvents and Reagents 601-10 1/94,Potential Problems 601-10 1/94,Specific Solvents 601-12 1/94,Chapter 1,Regulatory Operations,Chapter 2,General Analytical,Operations and Information,Chapter 3,Multiclass,MRMs,Chapter 5,GLC,Chapter 4,Selective,MRMs,Chapter 6,HPLC,Transmittal No. 96-E1 (9/96),600–2 Form FDA 2905a (6/92),SECTION 600 Pesticide Analytical Manual Vol. I,page date,Reagent Blanks 601-14 1/94,Safety Precautions 601-14 1/94,601 E: Sample Preparation 601-14 1/94,Sample Cleanup 601-14 1/94,Sample Filtration 601-14 1/94,Sample Solvent Degassing 601-15 1/94,Choice of Sample Solvent 601-15 1/94,601 F: Reference Standards 601-15 1/94,Stock Solutions 601-15 1/94,Working Standard Solutions 601-16 1/94,Storage 601-16 1/94,References 601-16 1/94,602: Columns,602 A: Column Selection 602-1 1/94,602 B: Analytical Columns 602-1 1/94,Liquid-Solid Chromatography 602-2 1/94,Bonded Phases 602-2 1/94,Ion Exchange 602-3 1/94,Ion Pair 602-4 1/94,Size Exclusion 602-4 1/94,602 C: Column Evaluation 602-5 1/94,602 D: Column Specifications 602-6 1/94,602 E: Analytical Column Protection 602-8 1/94,Filters 602-8 1/94,Precolumns 602-9 1/94,Guard Columns 602-9 1/94,602 F: Column Maintenance and Troubleshooting 602-9 1/94,Column Care 602-9 1/94,Column Evaluation by Injection of 602-10 1/94,Test Mixtures,Column Storage 602-11 1/94,Column Regeneration 602-11 1/94,References 602-12 1/94,603: Mobile Phase Selection, Preparation, and Delivery,603 A: Mobile Phase Selection 603-1 1/94,Normal Phase Chromatography 603-1 1/94,Reverse Phase Chromatography 603-3 1/94,Ion Exchange Chromatography 603-4 1/94,Ion Pair Chromatography 603-5 1/94,Size Exclusion Chromatography 603-5 1/94,Gradient Elution in HPLC 603-5 1/94,603 B: Mobile Phase Preparation 603-6 1/94,Filtering Solvents 603-6 1/94,Degassing Solvents 603-6 1/94,Transmittal No. 96-E1 (9/96),Form FDA 2905a (6/92) 600–3,Pesticide Analytical Manual Vol. I SECTION 600,page date,Solvent Reservoirs 603-7 1/94,603 C: Mobile Phase Delivery Systems 603-8 1/94,Pumps 603-8 1/94,Gradient Programming Systems 603-10 1/94,603 D: Maintenance and Troubleshooting 603-10 1/94,Problems with Pumps 603-10 1/94,References 603-13 1/94,604: Injection Systems,604 A: Injection Valves 604-1 1/94,604 B: Automatic Injectors 604-3 1/94,604 C: Operation, Maintenance, Troubleshooting, 604-3 1/94,and Repair of Injection Valves,References 604-4 1/94,605: Detectors,605 A: UV/VIS Absorbance Detectors 605-2 1/94,Fixed Wavelength UV Detectors 605-3 1/94,Variable Wavelength UV Detectors 605-4 1/94,Solvents 605-4 1/94,Performance Characteristics 605-4 1/94,Multichannel or Photodiode Array Detectors 605-5 1/94,Applications 605-5 1/94,Problems, Maintenance, and 605-5 1/94,Troubleshooting,605 B: Fluorescence Detectors 605-6 1/94,Detector Design 605-6 1/94,Solvents 605-7 1/94,Performance Characteristics 605-7 1/94,Parameter Adjustments 605-8 1/94,Applications 605-8 1/94,Detector Maintenance 605-8 1/94,605 C: Electrochemical Detectors 605-8 1/94,Conductivity Detectors 605-9 1/94,Amperometric and Coulometric Detectors 605-9 1/94,Performance Characteristics 605-10 1/94,Applications 605-11 1/94,605 D: Photoconductivity Detectors 605-11 1/94,Apparatus 605-11 1/94,Performance Characteristics 605-11 1/94,Applications 605-13 1/94,605 E: Mass Spectrometric Detectors 605-13 1/94,605 F: Derivatization for Detection Enhancement 605-14 1/94,Comparison of Pre- and Post-Column 605-14 1/94,Derivatization,Transmittal No. 96-E1 (9/96),600–4 Form FDA 2905a (6/92),SECTION 600 Pesticide Analytical Manual Vol. I,page date,Post-Column Reactor Design 605-14 1/94,References 605-16 1/94,606: Residue Identification and Quantitation,606 A: Residue identification 606-1 1/94,Co-chromatography 606-1 1/94,Use of Alternative Columns 606-2 1/94,Spectrometric Confirmation 606-2 1/94,606 B: Quantitation 606-3 1/94,Reference 606-3 1/94,607: Quality Assurance and Troubleshooting,Performance Testing,608: Bibliography,General Texts 608-1 1/94,Columns 608-1 1/94,Detectors 608-2 1/94,Troubleshooting 608-2 1/94,Application to Pesticides 608-2 1/94,Figures,601-a Chromatographic Separation Techniques 601-1 1/94,601-b HPLC Modes of Operation 601-2 1/……
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